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CM3215
Fundamentals of Chemical Engineering Laboratory


Guidelines on Laboratory Notebooks
Dr. Faith Morrison
12 January 2014

Laboratory notebooks are a permanent record of what went on in the laboratory.  They have three important purposes.

Purposes of the laboratory notebook:
1.  accurately record data and observations for you to use in preparing your calculations and report.  It is impossible to remember everything that goes on in the lab day after day.  That's why we write down a record.
2.  provide a time-stamp of what was done when in case a safety or other inquiry is conducted.  The laboratory notebook is sequential (that's why it's bound) so that the order that steps were performed can be determined from the lab notebook record.
3.  provide a time-stamp of what was done in case of filing a patent record of invention.  The sequence and timing of discoveries can be determined from the laboratory notebook record.  This can have important legal implications.

Lab notebooks will be assessed at the beginning of the Monday lecture weekly.
Prelab assignments must be completed in your laboratory notebooks; these will be checked at the beginning of the Monday lecture, weekly.
The goal of the laboratory notebook is to be a repository of all the information about the laboratory work you are performing. 

The laboratory notebook contains:
1.  Safety information.  This should be easy to find and use to keep the laboratory safe.
2.  Your prelab calculations and preparations
3.  Everything you write down in the lab.  Examples include:  rough sketches, instructions from TA/instructor, data, temperatures, observations.
4.  Calibration curves that you determine that you will need in future labs.  Print a graph of the calibration curve with the equation shown and tape it securely into the lab notebook.
5.  Notes of discussions with your lab partners.
6.  Observations related to the experiments you are conducting.  If you find yourself asking "I wonder if I should note this down?" the answer is yes, note it down. Examples include:  whistling sounds, difficulty in turning a valve, room temperature, time of day, strange colors, strange odors, questions for the TA/instructor, suggestions for improvements, difficulties you experience.
7.  Final plots of your data (optional, but very helpful).  The CM3215 lab sessions build upon one another.  You will need the results from early lab in later labs.  It will be very convenient to have the plots in your laboratory notebook.
8.  Anything pertaining to the lab that you wish to put into the notebook.

In terms of style, for laboratory notebook:
1.  Everything is written in blue or black pen (pencil marks can smudge and become unreadable; red, green, purple ink fade with time).
2.  Every entry or at least every page is dated and initialled by the person making the entry.
3.  Writing is neat.
4.  Nothing is erased:  neatly cross out things (with a straight-edge ruler if possible) you wish to correct and neatly write the corrections nearby or indicate the page where the correction appears.  One diagonal line is sufficient to cross out an entire page.
5.  Papers may be affixed to the pages of your lab notebook (computer printouts for tables, for example) but you must completely outline them with cellophane tape so that all edges are taped down.  Do not use staples.  Do not allow pages to flap.
6.  Pages are numbered.
7.  There is a complete table of contents in the front (leave space on pages 1 and 2)
8.  Make sure the text of your entries are clear, not obscure. For example, do not just write "21oC" but rather write "room temperature at 9:15am =21oC"

Please think of the laboratory notebook assignment in this class as a process. We are working together to teach you how to keep a laboratory notebook. When we grade your notebook, we are looking to see that you are picking up on the instructions we are giving you. We are not requiring that you have a pristine laboratory notebook at all times. Therefore, if something is wrong in your notebook, cross out the page and re-do it on the next available page. Indicate on the first page the page number where the re-do may be found.  Never remove pages from your bound laboratory notebook.

More information on lab notebooks
1. your name must be on it.
2. to prepare for a given week's lab, you must produce a safety section identifying the typical hazards.
3. to prepare for a given week's lab, reasonable data tables must be prepared in the lab notebook, with expected units indicated.
4. any questions assigned in the lab instructions (these are on the cm3215 web page) must be included.
5.  look up any physical property data you will need (heat capacity, densities, etc.) and record it and the reference in your lab notebook.
6.  Print off the unit conversion sheet from the class website and affix it to the back of your laboratory notebook:  www.chem.mtu.edu/%7Efmorriso/cm310/convert.pdf




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