Topic #
(usually wk) |
topic |
notes |
Lab Procedures |
Assignment
Instructions |
Handouts |
1 |
Laboratory Orientation (Visio P&ID) |
none |
Assignment 1:
Create a P&ID for the laboratory station
updated 10Jan2016 Excel In-lab exercise 1 updated 10Jan2016 |
||
2 |
Calibrate Honeywell Differential Pressure Cell |
Lecture: Calibrate
DP Meter updated 13Jan2016 Statistics 1 Random Error and Replicates updated 20Jan2016 |
Procedure:
Calibrate the DP Meter updated 13Jan16 |
Replicate
Error In-lab exercise 2 updated 21Jan2016 How to get Excel to display 95% CI error bars updated 23Jan2015 |
Schematic of set-up SDS Blue Fluid (Safety Data Sheet) SDS Acetone (Safety Data Sheet) Pycnometer accuracy pycnometer receipt ($173.31 each 2011) 10 mL and 25 mL sizes are for ASTM Standard D 369 and Barrett test H-8; AASHTO standard T-74 Accuracy of Volumetric Glassware Technical Specifications Honeywell STD924 archived Appendix rules 1 Appendix rules 2 Hints on how to insert figures without a Basics Violation How to get Excel to display 95% CI error bars updated 23Jan2015 Instructions on Excel's LINEST -fittingto a line with LINEST updated 25Sept2014 -fitting to a polynomial with LINEST updated 26June2015 _______________________ Calibration Weights Lecture Pressure (handwritten slides 2009) Challenging manometer Plm |
3 |
Reading and Calibration Error |
Statistics
2: Reading Error
20Jan2016 Statistics 3 Calibration Error 26Jan2016
Also, see below under week 6 and on Dr. Morrison's Statistics page |
none |
Assignment 3: Reading
and Calibration Error
26Jan2016
|
see below under week 6 Reading and Calibration combined (print double sided) 1Aug19 |
4 |
Measure Solution Viscosity as a function of Concentration | Lecture: Viscosity
Measurement updated 25Jan2016 Google Forms link for data collection (Sp2016) updated 25Jan2016 Statistics 4. Error Propagation 1Feb2016 Also, see below under week 6 |
updated 25Jan2016
|
SDS Sucrose (Safety Data Sheet) Instructions for CF Viscometers Background on CF Viscometers (reference: F. A. Morrison, Department of Chemical Engineering, Michigan Technological University, Draft manuscript 2009, Houghton, MI) Lab CF Calibration Sheets Table of approximate efflux times updated 16Sept2014 Link to Perry's on-line for members of AIChE Confidence Intervals for Student's T iidea for 2012: active learning |
|
5 |
Calibrate Flowmeters and Explore Reynolds Number |
10Feb2016 5. Least Squares Curve Fitting and LINEST |
Procedure:
Calibrate Rotameter 10Feb2016 |
The
Copper Tube Handbook The Reynolds number is named after Osborne Reynolds |
|
6 |
Error Analysis in Engineering Applications Summary page: www.chem.mtu.edu/ ~fmorriso/statistics.html |
Lectures Statistics: (summary page) 1. Lecture: Random Error and Replicates 20Jan2015 2. Reading Error 20Jan2016 3. Calibration Error 26Jan2016
4. Error Propagation 1Feb2016 Excel 5. Least Squares Curve Fitting and LINEST 26Jan2016 6. Sensing Limit 26Jan2016 7. Practice --working with Error Propagation Guidelines for Evaluating and Expressing the Uncertainty of NIST Measurement Results (pdf; 1994)
|
none | Reading Error
Worksheet Replicate Error Worksheet Calibration Error Worksheet (2 pages) Error Propagation Worksheet Reading and Calibration combined (print double sided) 19Feb16 Confidence Intervals for Student's T 23Jan2015 How to get Excel to display 95% CI error bars updated 23Jan2015 Instructions on Excel's LINEST -fitting to a line with LINEST updated 25Sept2014 -fitting to a polynomial with LINEST updated 26June2015 Volumetric Glassware Error 11Sept2014 ____________________ Dr. Pintar's Unit Operations Lab handout on Error Analysis (2012) Dr. Co's 1996 Least Squares fitting handout Dr. Co's 2008 LINEST handout A statistics example from the KBC |
|
7 |
Characterization of a Pneumatic Control
Valve |
Lecture:
Control Valves updated 17Feb2016 |
Procedure: Characterize a
Control Valve 17 Feb2016 |
Assignment 5 (Attached to the Procedure) |
updated 18Nov13
(note: some of the information in this
handout is the same as for the System Curve assignment)
|
8 |
Friction/Re |
updated 24Feb2016
|
updated 24Feb2016
|
none |
The
Copper Tube Handbook The Moody Diagram, f(Re) |
9 |
System Curve
(Friction losses in a piping system) |
updated 2March2016
|
none |
Assignment 6: System Head Curves for a Piping System with a Needle Valve posted 2 March 2016 |
updated 18Nov13
|
10 |
Overall
Heat-Transfer Coefficient for a Double-Pipe Heat Exchanger |
updated 16Mar2016
|
Swagelok
Steam Trap Specs OPT Steam Trap Specs installed stations 3, 7 2015 Steam Tables SI units Dr. Morrison's CM2110 Energy Balance Notes hand lecture slides 11Nov2013 |
||
11 |
System Identification:
Fitting a Model to Data |
updated 28March2016
|
(No laboratory work;
data sets supplied) |
updated 28March2016
|
Model
Identification for Laboratory Data updated 30Nov2014 Appendix: Table 2: Analytical Functions updated 2Dec2014 Using Solver to Fit Curves What are RTDs? Carreau model data: fittingCarreau2010blank.xls |
12 |
Analysis of the "Lossy" Centrifugal Pump |
Lecture:
Pumping updated 30March2016 hand lecture slides 2013 |
Procedure:
Characterize the Lossy Pump updated 10March 2016 |
none |
Pumping Head
Handout Cv of Metering Valves - Morrison updated 18Nov13 |
13 |
Determining Heat Transfer Coefficient for a Solid Ball in a well stirred liquid in a finite vessel |
Lecture: Sphere
Heat Transfer updated 26 February 2019 |
(No laboratory work; data set supplied) |
Assignment 8:
Heat Transfer Coefficient for Sphere Spring 2016 Lab Data for Spring 2016 updated 8April2016 |
Heisler Chart Heisler 1947 article Analytical Solution (Carslaw and Jaeger) |
14 |
Week 14 Safety Quiz | Safety Notes Archive | |||
Finals |
none | none |